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Analysis of Maltose Starch Powder According to Japanese Pharmaceutical Excipients Method (KS-801)

Maltose starch powder was analyzed on SUGAR KS-801 according to Japanese Pharmaceutical Excipients 2013 method. It is necessary for the choice of
Column to satisfy resolution of maltotriose/maltose of ≥ 1.6 and maltose/glucose of ≥ 4.1. It was confirmed that resolution of maltotriose/maltose was more than 2.0 and that of maltose/glucose was more than 5.0 when they were analyzed using KS-801.

Sample : 5mg/mL each, 10µL
1. Maltotriose
2. Maltose
3. Glucose

Column : Shodex SUGAR KS-801 (8.0mmI.D. x 300mm)

Eluent : H2O

Flow rate : 0.4mL/min

Detector : Shodex RI

Column temp. : 50°C