GPC LF linear columns
with multi-pore gel
The GPC column with highly linear calibration curve
Product information
GPC LF-404, GPC LF-604, GPC LF-804
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Packed with unique multi-pore gels with a wide pore-size distribution
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Highly linear calibration curve without inflection points
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Achieves highly precise molecular weight distribution determination
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Enables analysis over a broad range of molecular weights
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Rapid analysis column (LF-604) and high performance analysis column (LF-404) are also available
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LF-604 and LF-404 enables reduction of solvent use
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Fulfills USP L21 requirements
2 to 4 columns can be connected in series according to separation purpose or samples.
Analytes: all polymers, which are soluble in one of the mentioned organic solvents
This column series has similar properties like the following references: Tosoh TSKgel Multipore Hxl-M
Product overview
Product code | Product name | Separation | Gel material | Plates per column | Particle size | Pore size | Size (ID x length) | Housing material |
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F6021043 | GPC LF-404 | GPC | Styrene divinylbenzene copolymer | ≥ 14,000 | 6 µm | 3,000 Å | 4.0 x 250 mm | steel |
F6021042 | GPC LF-604 | GPC | Styrene divinylbenzene copolymer | ≥ 9,000 | 6 µm | 3,000 Å | 6.0 x 150 mm | steel |
F6021041 | GPC LF-804 | GPC | Styrene divinylbenzene copolymer | ≥ 17,000 | 6 µm | 3,000 Å | 8.0 x 300 mm | steel |
F6709621 | GPC LF-G | GPC | Styrene divinylbenzene copolymer | (guard) | 6 µm | - | 4.6 x 10 mm | steel |
Product details
Product name | Maximum pressure | Usual flow rate | Maximum flow rate | Temperature range | Shipping solvent | USP | MW range | Exclusion limit |
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GPC LF-404 | 3.5 MPa (35 bar) | 0.3 mL/min | 0.6 mL/min | 20 to 60°C | THF | L21 | 300 - 2,000,000 | 2,000,000 |
GPC LF-604 | 3.5 MPa (35 bar) | 0.5 mL/min | 1.0 mL/min | 20 to 60°C | THF | L21 | 300 - 2,000,000 | 2,000,000 |
GPC LF-804 | 3.5 MPa (35 bar) | 1.0 mL/min | 2.0 mL/min | 20 to 60°C | THF | L21 | 300 - 2,000,000 | 2,000,000 |
GPC LF-G | - | - | - | 20 to 60°C | THF | L21 | - | - |
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Product instruction
Eluents:
The shipping solvent is Tetrahydrofuran (THF). The in-column solvent can be replaced. Following eluents are suitable:
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THF
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Chloroform
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Carbon tetrachloride
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Toluene
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Methyl ethyl ketone
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Acetone
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Dimethylformamide (DMF) Usable at 40°C or higher)
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Dimethylacetamide (DMAc) (Usable at 40°C or higher)
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Hexafluoroisopropanol (HFIP) (Usable at 40°C or higher)
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N-Methylpyrrolidone (NMP) (Usable at 40°C or higher)
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Dimethylsulfoxide (DMSO) (Usable at 40°C or higher)
Guard column:
The use of the guard column GPC LF-G is recommended.
Cleaning and Regeneration:
Clean the guard column and analytical column separately by running the eluent at 50% of standard flow rate in the opposite direction of the arrow on the column tag in order to remove the clogged substance.
Applications
Calibration Curve for LF-804 (DMAc Eluent: PEG, PEO)
Calibration Curve for LF-804 (DMAc Eluent: PS)
Calibration Curve for LF-804 (DMF Eluent: PEG, PEO)
Calibration Curve for LF-804 (DMSO/DMF Eluent: Pullulan)
Calibration Curve for LF-804 (Methyl Ethyl Ketone Eluent: PMMA)
Calibration Curve for LF-804 (NMP Eluent: PEG, PEO)
Calibration Curve for LF-804 (NMP Eluent: PS)
Calibration Curve for LF-804 (THF Eluent: PS)
Calibration Curve for LF-404 (HFIP Eluent: PMMA)
Calibration Curves for LF-404 and LF-604 (THF Eluent: PS)
Comparison of LF-804, LF-404 and LF-604
GPC LF-804 (8.0 x 300 mm)
Analysis of Polyhydroxybutyric Acid (LF-804)
Poly(2-Vinylpyridine-co-styrene) (LF-804)
Poly(4-Vinylpyridine) (LF-804)
Poly(Ethylene Oxid) and Poly(Ethylene Glycol) Standards (2) (LF-804)
Poly(Methyl Methacrylate) (2) (Eluent: Methyl Ethyl Ketone)
Poly(Vinyl Butyral) (2) (LF-804)
Poly(Vinyl Formal) (2) (LF-804)